journal6 ›› 2002, Vol. 23 ›› Issue (2): 90-92.

• Scientific research bulletin • Previous Articles     Next Articles

Preparation of the High-Pure Capsaicin Chemical Compound by Way of Extraction and Crystallization

  

  1. (1.Huang Shan Chong Breeding Farm of Guizhou Bus-manufacturing Plant,Guiyang  550003,China;2.The Life Science and Chemical Department of Jishou University,Jishou 416000,Hunan China)
  • Online:2002-06-15 Published:2013-01-05

Abstract: Use hot pepper as material,and dissolve it in the solution of 2% sodium hydroxide,after this,acidulate it with the solution of 5% H2SO4,extract with n-Hexane and concentrate it,then the crude product(its degree of purity is 82%~84%)of the capsaicin chemical compound is obtained.In the next step,dissolve the crude product in the mixed solution of n-Hexane-Hexyl acetate,then,after recrystallizing it,the crystal of the high-pure capsaicin chemical compound is obtained,it's degree of purity being 92.5%,according to the examination standard of GB10783—1996.The obtaining rate of the high-pure capsaicin chemical compound is 2.2%(relative to the element of hot pepper).

Key words: the element of hot pepper, capsaicin chemical compound, extraction, recrystallize

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