journal6 ›› 2008, Vol. 29 ›› Issue (4): 71-74.

• Chemistry and chemical engineering • Previous Articles     Next Articles

Synthesis of Cyclohexyl Acetate Catalyzed by Ferric Sulfate Hydrate under Microwave Irradiation


  1.  (College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000,Hunan China)
  • Online:2008-07-25 Published:2012-05-21

Abstract: Cyclohexyl acetate was synthesized by using ferric sulfate hydrate as catalyst under microwave irradiation.The optimum experimental condition was obtained as follows:the power of microwave irradiation was 640 W,molar ratio of alcohol to acid was 1.4∶1,the dosage of water-carring reagent was 6 mL,the amount of catalyst was 1.0 g,and the reaction time was 30 min.Under the optimum experimental condition,the yield of the product was 91.6% (based on acetic acid).

Key words: microwave irradiation, ferric sulfate hydrate, cyclohexyl acetate

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