journal6 ›› 2004, Vol. 25 ›› Issue (4): 49-52.

• 重点学科 • 上一篇    下一篇

月见草花黄色素提取工艺研究

  

  1. (1.吉首大学化学化工学院,湖南 吉首 416000;2.湘西州体育学校,湖南 吉首 416000)
  • 出版日期:2004-12-15 发布日期:2012-09-22
  • 作者简介:陈小原(1956-),女,湖南省吉首大学化学化工学院教授,主要从事天然产物与有机合成研究.
  • 基金资助:

    湖南省教育厅重点资助项目(02A037)

Study on Extraction Technology of Yellow Pigment From Oenothera Brennis L.Flower

  1. (1.Collage of Chemistry and Chemical Engineering,Jishou university,Jishou  416000,Hunan China;2.School of Physical Education of Western Hunan,Jishou 416000,Hunan China)
  • Online:2004-12-15 Published:2012-09-22

摘要:对月见草花黄色素的提取条件进行了系统的研究,比较了无水乙醇、95%乙醇、乙醚、丙酮、乙酸乙酯、石油醚提取月见草花黄色素的效果.结果显示:以95%乙醇为最佳溶剂,95%乙醇提取液的λmax为394 nm.单因素试验和正交试验表明,温度对提取月见草花黄色素的影响较大,而浸提时间和料液比影响较小.提取的最佳工艺条件是:以体积分数95%的乙醇为浸提剂,按每0.2 g月见草花粉末加浸提剂30 mL的比例投料,在温度60 ℃下,浸提时间为4 h.月

关键词: 见草花, 黄色素, 提取工艺

Abstract: The extraction conditions of yellow pigment from Oenothera brennis.L flower were studied.The extraction effects by pure ethanol,95% alcohol,ether,acetone,ethyl ethanoate,petroleum benzene were compared,and the result indicated that 95% alcohol was the optimum solvent.the maximum absorption wavelength(λmax) of the 95% alcohol being 394 nm.Mono-factor experiments and orthogonal experiments showed that the experiment temperature could have a greater impact on extraction of the yellow pigment than the ratio of the solvent to petal and extraction time of solvent.The result showed that the optimum conditions are the following:the extraction reagent 95% alcohol,the petal and 95% alcohol  were put in container with the ratio of 0.2∶30(g/mL) then heated at 60 ℃ for 4 h.

Key words: Oenothera brennis L.flower, yellow pigment, extraction technology

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