journal6 ›› 2002, Vol. 23 ›› Issue (2): 90-92.

• 科研简报 • 上一篇    下一篇

萃取-结晶法制备高纯辣椒碱类化合物

  

  1. (1.贵州省客车制造厂黄鳝冲养殖场,贵州 贵阳 550003;2.吉首大学生命科学与化学学院,湖南 吉首 416000)
  • 出版日期:2002-06-15 发布日期:2013-01-05
  • 作者简介:张世文(1964-),男,湖南省桑植县人,贵州省客车制造厂黄鳝冲养殖场副研究员,硕士研究生,主要从事天然有机物的提取、分离和应用研究.

Preparation of the High-Pure Capsaicin Chemical Compound by Way of Extraction and Crystallization

  1. (1.Huang Shan Chong Breeding Farm of Guizhou Bus-manufacturing Plant,Guiyang  550003,China;2.The Life Science and Chemical Department of Jishou University,Jishou 416000,Hunan China)
  • Online:2002-06-15 Published:2013-01-05

摘要:以辣素为原料,将其溶于2%的氢氧化钠溶液中,以5%的H2SO4溶液酸化,正己烷萃取并浓缩得纯度为82%以上的辣椒碱类化合物粗品.将粗品辣椒碱类化合物溶解于正己烷-乙酸已酯混合溶剂中,重结晶得纯度为92.5%的高纯辣椒碱类化合物晶体,平均得率2.24%(相对于辣素).

关键词: 辣素, 辣椒碱类化合物, 萃取, 重结晶

Abstract: Use hot pepper as material,and dissolve it in the solution of 2% sodium hydroxide,after this,acidulate it with the solution of 5% H2SO4,extract with n-Hexane and concentrate it,then the crude product(its degree of purity is 82%~84%)of the capsaicin chemical compound is obtained.In the next step,dissolve the crude product in the mixed solution of n-Hexane-Hexyl acetate,then,after recrystallizing it,the crystal of the high-pure capsaicin chemical compound is obtained,it's degree of purity being 92.5%,according to the examination standard of GB10783—1996.The obtaining rate of the high-pure capsaicin chemical compound is 2.2%(relative to the element of hot pepper).

Key words: the element of hot pepper, capsaicin chemical compound, extraction, recrystallize

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