journal6 ›› 2015, Vol. 36 ›› Issue (4): 59-63.DOI: 10.3969/j.cnki.jdxb.2015.04.015

• 特色专栏.武陵山片区研究 • 上一篇    下一篇

猕猴桃亚麻酸油纳米乳剂的制备工艺

张永康, 胡江宇, 欧阳辉, 沈国励, 陈功锡, 王晓京力   

  1. (1.吉首大学植物资源保护与利用湖南省高校重点实验室,湖南 吉首 416000;2.湖南大学化学生物传感与计量学国家重点实验室,湖南 长沙 410082;3.湖南省猕猴桃产业化工程技术研究中心,湖南  吉首 416000 )
  • 出版日期:2015-07-25 发布日期:2015-07-27
  • 作者简介:张永康(1939—),男,浙江杭州人,吉首大学植物资源保护与利用湖南省高校重点实验室教授,博士生导师,主要从事植物化学及农业产业化开发研究.
  • 基金资助:

    湖南省高校产业化培育资助项目(10CY010)

Preparing Technology of Nanoemulsion with Kiwi Linolenic Acid Oil

 ZHANG Yongkang,HU Jiangyu,OUYANG Hui,SHEN Guoli,CHEN Gongxi,WANG Xiaoqing   

  1. (1. University Key  Laboratory of Plant Resources Conservation and Utilization(Hunan Province),Jishou University,Jishou 416000,Hunan China;2.State Key Laboratory of Chemo/Biosensing and Chemometrics,Hunan University,Changsha  410082,China;3.Hunan Kiwi Engineering and Industrialization Research Center,Jishou 416000,Hunan China)
  • Online:2015-07-25 Published:2015-07-27

摘要:利用自身研制的具有一定pH值的复合乳化剂,采用高速剪切乳化或纳米高压均质技术对猕猴桃亚麻酸油进行分散或均质,使猕猴桃亚麻酸形成具有纳米尺度的稳定的水包油颗粒,再运用纳米粒度及Zeta电位仪对其进行纳米粒径表征.以粒径小、稳定时间长为主要考察指标,得到制取猕猴桃亚麻酸油纳米乳剂的最佳工艺条件为乳化剂4 g,猕猴桃亚麻酸油4 mL,制备液体积200 mL,9 000 r/min剪切乳化20 min或150 MPa左右高压均质循环2次.研究结果表明,在最佳工艺条件下平均粒径为(60±10)nm,剪切乳化稳定时间约1.5 a,高压均质稳定时间达2 a以上,满足制药和保健品的需要.

关键词: 纳米乳剂, 猕猴桃, 亚麻酸油, 水包油, 剪切乳化, 高压均质

Abstract: Kiwi linolenic acid oil has been dispersed to form stable nano-scaled oil-in-water particulates with the independently-prepared compound emulsifier with definite pH through high speed shearing,emulsification and high pressure homogenizing technique.According to the nano granularity,the particulate diameter has been represented by Zeta.The results showed that with 4 g emulsifier,4 mL Kiwi linolenic acid oil,200 mL preparation solution,9 000 r/min shearing and emulsification for 20 min or two times of 150 MPa high pressure homogeneity circulation,the average minimum particulate diameter was (60±10)nm and the average maximum stable durations for shearing and emulsification and for high pressure homogeneity were 1.5 a and more than 2 a respectively. Such technological condition is the optimum and can satisfy pharmacy and health food industry.

Key words: nanoemulsion, kiwi, linolenic acid oil, oil-in-water, shearing and emulsification, high pressure homogenization

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