液相法制备纳米氧化锌的研究( Ⅰ)

journal6 ›› 2000, Vol. 21 ›› Issue (2): 9-11.

液相法制备纳米氧化锌的研究( Ⅰ)

( 1.吉首大学生命科学与化学学院,湖南吉首 416000; 2. 湘西州外贸化工厂,湖南吉首 416000)

出版日期:2000-06-15 发布日期:2013-01-16
作者简介:刘建本( 1955~ ) ,女, 吉首大学生命科学与化学学院副教授,主要从事无机材料方面的研究.
基金资助:
湖南省自然科学基金资助项目( 99JJY2071)

Nanosized Zinc Oxide Prepared by Liquid- phase Precipitation

(1.College of Life Science and Chemistry, Jishou University, Jishou 416000, Hunan China;2.Chemical Industry Factory of Foreign Trade, Jishou 416000, Hunan China)

Online:2000-06-15 Published:2013-01-16

摘要/Abstract

摘要：以 ZnSO₄•7H₂O 和( NH₄) ₂CO₃ 为原料,添加表面活性剂, 在室温下、水溶液中沉淀出碳酸锌胶状沉淀, 经洗涤干燥后在200 热分解, 得到纳米氧化锌粉末,经XRD和TEM检测,粒径为5.7 nm.

关键词： 纳米氧化锌, 碳酸锌, 液相法

Abstract: By using ZnSO₄•7H₂O and (NH₄)₂CO₃ as materials, Zinc carbonate colloid was obtained in water at room temperature with presence of surface active reagent , then Nanocrystalline ZnO was produced by decomposed after washing and desiccated. Nanosized Zinc Oxide was characterized by X-ray powder diffraction ( XRD) and transmission electron microscope ( TEM) . XRD and TEM show that ZnO crystalline is spherical particle with hexagonal structure,
the average diameter size is 5. 7 nm.

Key words: nanocyystalline Zinc oxide, Liquid phase, precipitation

刘建本, 易保华, 肖卓炳, 陈德根, 陈上, 张永康. 液相法制备纳米氧化锌的研究( Ⅰ)[J]. journal6, 2000, 21(2): 9-11.

LIU Jian-Ben, YI Bao-Hua, XIAO Zhuo-Bing, CHEN De-Gen, CHEN Shang, ZHANG Yong-Kang. Nanosized Zinc Oxide Prepared by Liquid- phase Precipitation[J]. journal6, 2000, 21(2): 9-11.