溶胶- 凝胶前体法制备纳米ZnO

journal6 ›› 2001, Vol. 22 ›› Issue (1): 75-77.

溶胶- 凝胶前体法制备纳米ZnO

(延安大学化学化工系, 陕西延安 716000)

出版日期:2001-03-15 发布日期:2013-01-05
作者简介:李东升( 1969- ) ,男, 陕西延安人,理学硕士, 延安大学化学化工系讲师, 主要从事纳米材料方面的研究.
基金资助:
陕西省自然科学基金资助项目( 2000H16) ; 陕西省教育厅科研专项基金资助项目( 96JK055, 00JK133)

The Preparation of Nanometer Zinc Oxide by Sol-Gel Precursor Method

( Dept. of Chemistry and Chemical Engineering, Yan’an University, Yan’an 716000, Shan’xi China)

Online:2001-03-15 Published:2013-01-05

摘要/Abstract

摘要：分别采用硬脂酸、柠檬酸及草酸盐Sol-Gel 法合成了干凝胶前体粉末,并以其热分析结果为依据,在指定温度下热处理2 h得ZnO粉体. 经XRD和SEM分析表明,三种方法均可制得具有六方晶系结构的纳米ZnO, 其中第一种方法所得粉体的结晶度好,团聚较轻, 粒子大小均匀,外貌呈球形.

关键词： 溶胶- 凝胶法, 前驱体, 纳米ZnO

Abstract: The powders of gel precursors were prepared by using the stearic acid, the citric acid and oxalate gel methods, respectively.And nanometer ZnO was obtained through calcination at the appointing temperature base on the data of thermal analysis of the gel precursors.The XRD and SEM showed that the three methods could be used to synthesise hexagonal ZnO nanometer powder, compare with other methods, ZnO nanometer powder prepared by the first method has higher crystal linity, better dispersity with sphere-shaped.

Key words: Sol-gel method, precursor, nanometer ZnO

李东升, 史振民, 秦振平, 王文亮, 王继武. 溶胶- 凝胶前体法制备纳米ZnO[J]. journal6, 2001, 22(1): 75-77.

LI Dong-Sheng, SHI Zhen-Min, QIN Zhen-Ping, WANG Wen-Liang, WANG Ji-Wu. The Preparation of Nanometer Zinc Oxide by Sol-Gel Precursor Method[J]. journal6, 2001, 22(1): 75-77.